Vanadium(V) Tartrato Complexes:  Speciation in the H 3 O + (OH - )/H 2 VO 4- /(2 R ,3 R )-Tartrate System and X-ray Crystal Structures of Na 4 [V 4 O 8 ( rac -tart) 2 ]·12H 2 O and (NEt 4 )